Viridis色譜柱提供了更多的非手性SFC選擇性。這些色譜柱基于的亞乙基橋雜化顆粒BEH、表面帶電雜化顆粒CSH、以及高強度硅膠顆粒HSS技術(shù)。 Viridis顆粒提供減少了的、且可控的表面硅醇基活性,從而為SFC分析分離提供 了峰形,即便對于保留的堿性非手性化合物也是如此。
使用超高效合相色譜(UPC2 )進行膠囊分析
(FSV)(通常來自充油膠囊、充粉膠囊或壓縮片粒)的分 析是一項具有挑戰(zhàn)性的任務(wù)。見的情況是,這些配方的分析都 采用正相色譜法,使用傳統(tǒng)的正相溶劑(己烷、叔丁醇、乙酸乙酯、 二氯甲烷等),采購和處理的成本相當高。用于FSV分析的其它分析色 譜技術(shù)包括反相液相色譜法、氣相色譜法、薄層色譜法和比色技術(shù)。 超高效合相色譜(UPC2 ™)為分析提供了一種可行的技術(shù), 它是一種具備成本效益的、可持續(xù)的和綠色環(huán)保的替代技術(shù),降低了 有機溶劑的用量,分析時間快,保持了色譜數(shù)據(jù)的品質(zhì)。使用 ACQUITY UPC2 系統(tǒng)分析了一系列FSV配方。被檢驗的配方有:、 +D3、,3、1和2,如表1所示。 這些實驗的結(jié)果表明,UPC2 有可能替代當今正在使用的許多分離方法 成為的一種技術(shù)。
品名 | 編號 |
Viridis BEH 2-Ethylpyridine Column, 130?, 5 µm, 2.1 mm X 150 mm, 1/pkg | 186006545 |
Viridis BEH 2-Ethylpyridine Column, 130?, 1.7 µm, 3 mm X 50 mm, 1/pkg | 186006580 |
Viridis BEH 2-Ethylpyridine Column, 130?, 1.7 µm, 3 mm X 75 mm, 1/pkg | 186006581 |
Viridis BEH 2-Ethylpyridine Column, 130?, 3.5 µm, 3 mm X 150 mm, 1/pkg | 186006659 |
Viridis BEH 2-Ethylpyridine Column, 130?, 3.5 µm, 3 mm X 100 mm, 1/pkg | 186006658 |
Viridis BEH 2-Ethylpyridine Column, 130?, 3.5 µm, 3 mm X 75 mm, 1/pkg | 186006657 |
Viridis BEH 2-Ethylpyridine Column, 130?, 3.5 µm, 3 mm X 50 mm, 1/pkg | 186006656 |
Viridis BEH 2-Ethylpyridine Column, 130?, 5 µm, 3 mm X 100 mm, 1/pkg | 186005751 |
Viridis BEH 2-Ethylpyridine Column, 130?, 5 µm, 3 mm X 50 mm, 1/pkg | 186005750 |
Viridis BEH 2-Ethylpyridine Column, 130?, 5 µm, 3 mm X 250 mm, 1/pkg | 186005753 |
Viridis BEH 2-Ethylpyridine Column, 130?, 5 µm, 3 mm X 150 mm, 1/pkg | 186005752 |
Viridis BEH 2-Ethylpyridine Column, 130?, 1.7 µm, 3 mm X 100 mm, 1/pkg | 186006582 |
Viridis BEH 2-Ethylpyridine Column, 130?, 5 µm, 4.6 mm X 50 mm, 1/pkg | 186005754 |
Viridis BEH 2-Ethylpyridine Column, 130?, 5 µm, 4.6 mm X 100 mm, 1/pkg | 186005755 |
Viridis BEH 2-Ethylpyridine Column, 130?, 5 µm, 4.6 mm X 150 mm, 1/pkg | 186005756 |
Viridis BEH 2-Ethylpyridine Column, 130?, 5 µm, 4.6 mm X 250 mm, 1/pkg | 186005757 |
Viridis BEH 2-Ethylpyridine Column, 130?, 3.5 µm, 2.1 mm X 100 mm, 1/pkg | 186006654 |
Viridis BEH 2-Ethylpyridine Column, 130?, 3.5 µm, 2.1 mm X 150 mm, 1/pkg | 186006655 |
Viridis BEH 2-Ethylpyridine Column, 130?, 3.5 µm, 2.1 mm X 50 mm, 1/pkg | 186006652 |
Viridis BEH 2-Ethylpyridine Column, 130?, 3.5 µm, 2.1 mm X 75 mm, 1/pkg | 186006653 |
Viridis BEH 2-Ethylpyridine Column, 130?, 1.7 µm, 2.1 mm X 75 mm, 1/pkg | 186006577 |
Viridis BEH 2-Ethylpyridine OBD Prep Column, 130?, 5 µm, 10 mm X 250 mm, 1/pkg | 186008259 |
Viridis BEH 2-Ethylpyridine Column, 130?, 1.7 µm, 2.1 mm X 100 mm, 1/pkg | 186006578 |
Viridis BEH 2-Ethylpyridine Column, 130?, 1.7 µm, 2.1 mm X 50 mm, 1/pkg | 186006576 |
Viridis BEH 2-Ethylpyridine Column, 130?, 1.7 µm, 3 mm X 150 mm, 1/pkg | 186006688 |
Viridis BEH Column, 130?, 1.7 µm, 2.1 mm X 100 mm, 1/pkg | 186006560 |
Viridis BEH Column, 130?, 1.7 µm, 3 mm X 75 mm, 1/pkg | 186006563 |
Viridis BEH 2-Ethylpyridine OBD Prep Column, 130?, 5 µm, 30 mm X 250 mm, 1/pkg | 186005770 |
Viridis BEH 2-Ethylpyridine OBD Prep Column, 130?, 5 µm, 50 mm X 50 mm, 1/pkg | 186005771 |
Viridis BEH 2-Ethylpyridine OBD Prep Column, 130?, 5 µm, 50 mm X 100 mm, 1/pkg | 186005772 |
Viridis BEH Column, 130?, 1.7 µm, 3 mm X 100 mm, 1/pkg | 186006564 |
Viridis BEH 2-Ethylpyridine OBD Prep Column, 130?, 5 µm, 50 mm X 150 mm, 1/pkg | 186005773 |
Viridis BEH 2-Ethylpyridine OBD Prep Column, 130?, 5 µm, 50 mm X 250 mm, 1/pkg | 186005774 |
Viridis BEH Column, 130?, 3.5 µm, 2.1 mm X 50 mm, 1/pkg | 186006634 |
Viridis BEH Column, 130?, 3.5 µm, 2.1 mm X 100 mm, 1/pkg | 186006636 |
Viridis BEH 2-Ethylpyridine Prep Guard Cartridge, 130?, 5 µm, 30 mm X 10 mm, 1/pkg | 186006909 |
Viridis BEH Column, 130?, 3.5 µm, 2.1 mm X 150 mm, 1/pkg | 186006637 |
Viridis BEH 2-Ethylpyridine VanGuard Pre-column, 130?, 3.5 µm, 2.1 mm X 5 mm, 3/pkg | 186006651 |
Viridis BEH 2-Ethylpyridine OBD Prep Column, 130?, 5 µm, 19 mm X 100 mm, 1/pkg | 186005763 |
Viridis BEH 2-Ethylpyridine OBD Prep Column, 130?, 5 µm, 19 mm X 150 mm, 1/pkg | 186005764 |
Viridis BEH 2-Ethylpyridine OBD Prep Column, 130?, 5 µm, 19 mm X 50 mm, 1/pkg | 186005762 |
Viridis BEH 2-Ethylpyridine VanGuard Pre-column, 130?, 1.7 µm, 2.1 mm X 5 mm, 3/pkg | 186006575 |
Viridis BEH Column, 130?, 1.7 µm, 2.1 mm X 75 mm, 1/pkg | 186006559 |
Viridis BEH 2-Ethylpyridine OBD Prep Column, 130?, 5 µm, 30 mm X 100 mm, 1/pkg | 186005768 |
Viridis BEH 2-Ethylpyridine OBD Prep Column, 130?, 5 µm, 30 mm X 75 mm, 1/pkg | 186005767 |
Viridis BEH 2-Ethylpyridine OBD Prep Column, 130?, 5 µm, 30 mm X 50 mm, 1/pkg | 186005766 |
Viridis BEH 2-Ethylpyridine OBD Prep Column, 130?, 5 µm, 19 mm X 250 mm, 1/pkg | 186005765 |
Viridis BEH Column, 130?, 1.7 µm, 2.1 mm X 50 mm, 1/pkg | 186006558 |
Viridis BEH Column, 130?, 1.7 µm, 3 mm X 150 mm, 1/pkg | 186006686 |
Viridis BEH 2-Ethylpyridine OBD Prep Column, 130?, 5 µm, 30 mm X 150 mm, 1/pkg | 186005769 |
Viridis BEH Column, 130?, 5 µm, 2.1 mm X 150 mm, 1/pkg | 186006544 |
Viridis BEH OBD Prep Column, 130?, 5 µm, 19 mm X 50 mm, 1/pkg | 186005731 |
Viridis BEH OBD Prep Column, 130?, 5 µm, 19 mm X 100 mm, 1/pkg | 186005732 |
Viridis BEH OBD Prep Column, 130?, 5 µm, 19 mm X 150 mm, 1/pkg | 186005733 |
Viridis BEH OBD Prep Column, 130?, 5 µm, 19 mm X 250 mm, 1/pkg | 186005734 |
Viridis BEH OBD Prep Column, 130?, 5 µm, 30 mm X 50 mm, 1/pkg | 186005735 |
Viridis BEH OBD Prep Column, 130?, 5 µm, 30 mm X 75 mm, 1/pkg | 186005736 |
Viridis BEH OBD Prep Column, 130?, 5 µm, 30 mm X 100 mm, 1/pkg | 186005737 |
Viridis BEH OBD Prep Column, 130?, 5 µm, 30 mm X 150 mm, 1/pkg | 186005738 |
Viridis BEH OBD Prep Column, 130?, 5 µm, 30 mm X 250 mm, 1/pkg | 186005739 |
Viridis BEH Column, 130?, 3.5 µm, 2.1 mm X 75 mm, 1/pkg | 186006635 |
Viridis BEH Column, 130?, 3.5 µm, 3 mm X 50 mm, 1/pkg | 186006638 |
Viridis BEH Column, 130?, 3.5 µm, 3 mm X 75 mm, 1/pkg | 186006639 |
Viridis BEH Column, 130?, 3.5 µm, 3 mm X 100 mm, 1/pkg | 186006640 |
Viridis BEH Column, 130?, 5 µm, 3 mm X 50 mm, 1/pkg | 186005719 |
Viridis BEH Column, 130?, 3.5 µm, 3 mm X 150 mm, 1/pkg | 186006641 |
Viridis BEH OBD Prep Column, 130?, 5 µm, 50 mm X 100 mm, 1/pkg | 186005741 |
Viridis BEH Column, 130?, 5 µm, 3 mm X 100 mm, 1/pkg | 186005720 |
Viridis BEH Column, 130?, 5 µm, 4.6 mm X 50 mm, 1/pkg | 186005723 |
Viridis BEH Column, 130?, 5 µm, 4.6 mm X 100 mm, 1/pkg | 186005724 |
Viridis BEH Column, 130?, 5 µm, 3 mm X 150 mm, 1/pkg | 186005721 |
Viridis BEH Column, 130?, 5 µm, 3 mm X 250 mm, 1/pkg | 186005722 |
Viridis BEH Fluoro Phenyl Prep Guard Cartridge, 130?, 5 µm, 30 mm X 10 mm, 1/pkg | 186006911 |
Viridis BEH Column, 130?, 5 µm, 4.6 mm X 150 mm, 1/pkg | 186005725 |
Viridis BEH Column, 130?, 5 µm, 4.6 mm X 250 mm, 1/pkg | 186005726 |
Viridis CSH Fluoro-Phenyl Column, 130?, 5 µm, 2.1 mm X 150 mm, 1/pkg | 186006543 |
Viridis CSH Fluoro-Phenyl Column, 130?, 1.7 µm, 2.1 mm X 50 mm, 1/pkg | 186006567 |
Viridis BEH VanGuard Pre-column, 130?, 3.5 µm, 2.1 mm X 5 mm, 3/pkg | 186006633 |
Viridis CSH Fluoro-Phenyl Column, 130?, 5 µm, 3 mm X 100 mm, 1/pkg | 186005689 |
Viridis CSH Fluoro-Phenyl Column, 130?, 1.7 µm, 2.1 mm X 75 mm, 1/pkg | 186006568 |
Viridis CSH Fluoro-Phenyl Column, 130?, 1.7 µm, 2.1 mm X 100 mm, 1/pkg | 186006569 |
Viridis CSH Fluoro-Phenyl Column, 130?, 3.5 µm, 3 mm X 150 mm, 1/pkg | 186006650 |
Viridis CSH Fluoro-Phenyl Column, 130?, 1.7 µm, 2.1 mm X 150 mm, 1/pkg | 186006570 |
Viridis CSH Fluoro-Phenyl Column, 130?, 5 µm, 3 mm X 150 mm, 1/pkg | 186005690 |
Viridis CSH Fluoro-Phenyl Column, 130?, 3.5 µm, 2.1 mm X 75 mm, 1/pkg | 186006644 |
Viridis CSH Fluoro-Phenyl Column, 130?, 3.5 µm, 2.1 mm X 50 mm, 1/pkg | 186006643 |
Viridis BEH OBD Prep Column, 130?, 5 µm, 50 mm X 150 mm, 1/pkg | 186005742 |
Viridis BEH OBD Prep Column, 130?, 5 µm, 50 mm X 50 mm, 1/pkg | 186005740 |
Viridis CSH Fluoro-Phenyl Column, 130?, 1.7 µm, 3 mm X 100 mm, 1/pkg | 186006573 |
Viridis CSH Fluoro-Phenyl Column, 130?, 1.7 µm, 3 mm X 50 mm, 1/pkg | 186006571 |
Viridis CSH Fluoro-Phenyl Column, 130?, 1.7 µm, 3 mm X 75 mm, 1/pkg | 186006572 |
Viridis BEH OBD Prep Column, 130?, 5 µm, 50 mm X 250 mm, 1/pkg | 186005743 |
Viridis BEH Prep Guard Cartridge, 130?, 5 µm, 30 mm X 10 mm, 1/pkg | 186006910 |
Viridis CSH Fluoro-Phenyl Column, 130?, 3.5 µm, 3 mm X 50 mm, 1/pkg | 186006647 |
Viridis CSH Fluoro-Phenyl Column, 130?, 3.5 µm, 3 mm X 75 mm, 1/pkg | 186006648 |
Viridis BEH VanGuard Pre-column, 130?, 1.7 µm, 2.1 mm X 5 mm, 3/pkg | 186006557 |
Viridis CSH Fluoro-Phenyl Column, 130?, 3.5 µm, 2.1 mm X 100 mm, 1/pkg | 186006645 |
Viridis CSH Fluoro-Phenyl Column, 130?, 3.5 µm, 2.1 mm X 150 mm, 1/pkg | 186006646 |
Viridis CSH Fluoro-Phenyl Column, 130?, 1.7 µm, 3 mm X 150 mm, 1/pkg | 186006687 |
Viridis CSH Fluoro-Phenyl Column, 130?, 3.5 µm, 3 mm X 100 mm, 1/pkg | 186006649 |
Viridis CSH Fluoro-Phenyl OBD Prep Column, 130?, 5 µm, 30 mm X 250 mm, 1/pkg | 186005708 |
Viridis CSH Fluoro-Phenyl OBD Prep Column, 130?, 5 µm, 30 mm X 150 mm, 1/pkg | 186005707 |
Viridis CSH Fluoro-Phenyl OBD Prep Column, 130?, 5 µm, 50 mm X 50 mm, 1/pkg | 186005709 |
Viridis CSH Fluoro-Phenyl VanGuard Pre-column, 130?, 1.7 µm, 2.1 mm X 5 mm, 3/pkg | 186006566 |
Viridis CSH Fluoro-Phenyl OBD Prep Column, 130?, 5 µm, 19 mm X 50 mm, 1/pkg | 186005700 |
Viridis CSH Fluoro-Phenyl OBD Prep Column, 130?, 5 µm, 19 mm X 150 mm, 1/pkg | 186005702 |
Viridis CSH Fluoro-Phenyl OBD Prep Column, 130?, 5 µm, 19 mm X 100 mm, 1/pkg | 186005701 |
Viridis CSH Fluoro-Phenyl OBD Prep Column, 130?, 5 µm, 30 mm X 50 mm, 1/pkg | 186005704 |
Viridis CSH Fluoro-Phenyl OBD Prep Column, 130?, 5 µm, 19 mm X 250 mm, 1/pkg | 186005703 |
Viridis CSH Fluoro-Phenyl OBD Prep Column, 130?, 5 µm, 30 mm X 100 mm, 1/pkg | 186005706 |
Viridis CSH Fluoro-Phenyl OBD Prep Column, 130?, 5 µm, 30 mm X 75 mm, 1/pkg | 186005705 |
Viridis CSH Fluoro-Phenyl Column, 130?, 5 µm, 3 mm X 50 mm, 1/pkg | 186005688 |
Viridis HSS C18 SB Column, 100?, 1.8 µm, 2.1 mm X 50 mm, 1/pkg | 186006617 |
Viridis HSS C18 SB Column, 100?, 1.8 µm, 2.1 mm X 75 mm, 1/pkg | 186006618 |
Viridis HSS C18 SB Column, 100?, 1.8 µm, 2.1 mm X 100 mm, 1/pkg | 186006619 |
Viridis HSS C18 SB Column, 100?, 1.8 µm, 2.1 mm X 150 mm, 1/pkg | 186006620 |
Viridis CSH Fluoro-Phenyl VanGuard Pre-column, 130?, 3.5 µm, 2.1 mm X 5 mm, 3/pkg | 186006642 |
Viridis CSH Fluoro-Phenyl Column, 130?, 5 µm, 4.6 mm X 250 mm, 1/pkg | 186005695 |
Viridis CSH Fluoro-Phenyl OBD Prep Column, 130?, 5 µm, 50 mm X 250 mm, 1/pkg | 186005712 |
Viridis CSH Fluoro-Phenyl OBD Prep Column, 130?, 5 µm, 50 mm X 150 mm, 1/pkg | 186005711 |
Viridis CSH Fluoro-Phenyl OBD Prep Column, 130?, 5 µm, 50 mm X 100 mm, 1/pkg | 186005710 |
Viridis CSH Fluoro-Phenyl Column, 130?, 5 µm, 3 mm X 250 mm, 1/pkg | 186005691 |
Viridis CSH Fluoro-Phenyl Column, 130?, 5 µm, 4.6 mm X 50 mm, 1/pkg | 186005692 |
Viridis CSH Fluoro-Phenyl Column, 130?, 5 µm, 4.6 mm X 100 mm, 1/pkg | 186005693 |
Viridis CSH Fluoro-Phenyl Column, 130?, 5 µm, 4.6 mm X 150 mm, 1/pkg | 186005694 |
Viridis Silica 2-Ethylpyridine Column, 100?, 5 µm, 3 mm X 250 mm, 1/pkg | 186005803 |
Viridis Silica 2-Ethylpyridine Column, 100?, 5 µm, 2.1 mm X 150 mm, 1/pkg | 186006542 |
Viridis Silica 2-Ethylpyridine Column, 100?, 5 µm, 3 mm X 150 mm, 1/pkg | 186005802 |
Viridis HSS C18 SB Column, 100?, 3.5 µm, 3 mm X 100 mm, 1/pkg | 186006631 |
Viridis HSS C18 SB Column, 100?, 3.5 µm, 3 mm X 75 mm, 1/pkg | 186006630 |
Viridis Silica 2-Ethylpyridine Column, 100?, 5 µm, 3 mm X 100 mm, 1/pkg | 186005801 |
Viridis Silica 2-Ethylpyridine OBD Prep Column, 100?, 5 µm, 19 mm X 150 mm, 1/pkg | 186004945 |
Viridis Silica 2-Ethylpyridine Column, 100?, 5 µm, 3 mm X 50 mm, 1/pkg | 186005800 |
Viridis HSS C18 SB Column, 100?, 3.5 µm, 3 mm X 150 mm, 1/pkg | 186006632 |
Viridis Silica 2-Ethylpyridine OBD Prep Column, 100?, 5 µm, 19 mm X 100 mm, 1/pkg | 186004944 |
Viridis HSS C18 SB VanGuard Pre-column, 100?, 1.8 µm, 2.1 mm X 5 mm, 3/pkg | 186006616 |
Viridis HSS C18 SB Column, 100?, 1.8 µm, 3 mm X 75 mm, 1/pkg | 186006622 |
Viridis HSS C18 SB Column, 100?, 1.8 µm, 3 mm X 50 mm, 1/pkg | 186006621 |
Viridis Silica 2-Ethylpyridine Column, 100?, 5 µm, 4.6 mm X 100 mm, 1/pkg | 186004936 |
Viridis Silica 2-Ethylpyridine Column, 100?, 5 µm, 4.6 mm X 50 mm, 1/pkg | 186004935 |
Viridis Silica 2-Ethylpyridine Column, 100?, 5 µm, 4.6 mm X 250 mm, 1/pkg | 186004938 |
Viridis Silica 2-Ethylpyridine Column, 100?, 5 µm, 4.6 mm X 150 mm, 1/pkg | 186004937 |
Viridis HSS C18 SB Column, 100?, 3.5 µm, 3 mm X 50 mm, 1/pkg | 186006629 |
Viridis HSS C18 SB Column, 100?, 3.5 µm, 2.1 mm X 100 mm, 1/pkg | 186006627 |
Viridis HSS C18 SB Column, 100?, 3.5 µm, 2.1 mm X 150 mm, 1/pkg | 186006628 |
Viridis HSS C18 SB Column, 100?, 3.5 µm, 2.1 mm
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